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FTIR, 1H NMR and 13C NMR spectra proved the structure of the copolymers and controllability of this new synthesis method.
Taken together, the results unequivocally proved the structure of OSCS as a polymer of the unusual tetrasulfonated disaccharide composed of 2,3- O-sulfoglucuronic acid and 4,6- O-sulfo N-acetylgalactosamine with a 1,3 linkage between the two sugars and 1,4 linkage between adjacent disaccharide units.
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Nuclear magnetic resonance spectroscopy (NMR), thermal gravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and transmission electron microscope (TEM) have been used to prove the structure of the hollow sphere and the intermediates.
The P NMR spectra of all four compounds prove the structure of the obtained compounds.
Finally, single crystal X-Ray diffraction studies prove the structures of our designed molecules.
However, attempts to geometry optimise both structures at the QM level proved unsuccessful, the structure of the partially optimised potassium containing G-quadruplex retains significant structural integrity with respect to the original crystal structure, whilst the sodium containing G-quadruplex significantficant structural distortion.
In [3], it has been proved that the structure of spatial time-frequency distribution matrix is similar to that of the traditional array covariance matrix.
It has been proved that the structure of α-Fe2O3 can be described as consisting hcp arrays of oxygen ions stacked along the [001] direction.
It was proved that the structure of diphenols in the diesterdianhydrides influences the cyclization which goes via an amino-imide to the imidazopyrrolone structure.
This study proved that the structure of eusynstyelamide was elucidated mistaken by Swersey et al. [129] and the authors have predicted the correct chemical structure of this compound and named as eusynstyelamide A. Both compounds 227, 228 showed neuronal nitric oxide synthase inhibition IC50 values of 4.3 5.8 µM.
Further analysis by Electrospray mass spectrometry (ESI-MS) proved that the structure of the purified product is correct (Fig 8).
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