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The oven temperature was held at 40°C for 5 min and then programmed to increase to 250°C at 10°C/min with a final 5 min hold at 250°C.
The column oven was maintained at 40°C for 3 min and then programmed to increase to 80°C at a rate of 1.5°C min−1.
The column oven was maintained at 40°C for 2 min and then programmed to increase to 130°C at a rate of 20°C/min.
The oven temperature was programmed to increase to 200°C at the rate of 10°C/min to hold at 200°C for 16 min and increase to 240°C at the rate of 60°C/min to hold at 240°C for 2 min. The total run time was just longer than 29 min. Helium was used as the carrier gas.
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The temperature program was as follows: the initial temperature was held at 100°C after injection, then programmed to increase at 1.5°C/min to 170°C (held there for 15 min), then programmed to increase at 0.5°C/min to 180°C (held there for 2 min), and finally to increase at 10°C/min to 215°C (held there for 20 min).
The oven temperature was held at 60°C for two minutes and programmed to increase at 10°C/minute from 60°C to 300°C and then held at 300°C for five minutes.
Incorporation of the new systems and enhancements caused the cost of the RAN carrier acquisition program to increase to AU£8.3 million.
The column temperature was programmed to increase from 40°C to 170°C with a linear gradient of 10°C/min.
The GC separation was performed under following conditions: oven temperature programmed to increase from 60 °C (5 min) to 180 °C (5 min) at a heating rate of 4 °C/min.
The column was programmed to increase from 135°C to 160°C at 2°C/min and from 160°C to 205°C at 1.5°C/min; the detection temperature was maintained at 220°C, injector temperature 220°C.
The gradient was programmed to increase from 53 to 58%% reservoir B (methanol) over 30 min.
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