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Various "in situ" techniques, including thermogravimetry (TG), differential thermal analysis (DTA), isothermal chemisorption, temperature-programmed desorption (TPD), intermittent TPD, temperature programmed reaction (TPR) and BET surface area determination, have been used to characterize calcium as a catalyst of carbon gasification.
Complementary continuous flow temperature programmed reaction experiments were also used.
The simulation predicts ignition and extinction transitions similar to those observed during a temperature programmed reaction experiment.
Thermal stability and products of decomposition of the adsorbed species were determined with temperature programmed reaction spectroscopy (TPRS) experiments.
A series of Mo nitride catalysts were prepared by the temperature programmed reaction of MoO3 with NH3.
Catalysts were characterized by temperature programmed reaction experiments in dry methane (TPR-CH4) followed by mass spectrometry.
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Operationally, it is a type of serial temperature-programmed reaction evaluation system.
The reaction dynamics and multiplicity features of CO oxidation on a Pt/SiO2 catalyst are studied via transient experiments combining Fourier transform infrared spectroscopy (FTIR) with temperature-programmed reaction (TPR) and with concentration-programmed reaction (CPR).
The optimized mechanism is validated against redundant experiments, including temperature-programmed desorption, temperature-programmed reaction, and molecular beam experiments.
CO hydrogenation over supported Rh catalysts was studied in an automatized microreactor by methods of parameter-programmed reaction.
Precise kinetic characterization, (non-steady-state and steady-state) was performed using pulse response methods, temperature-programmed reaction (TPR), etc.
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