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The programmed temperature enclosure was run at a programmed rate of 0.8 °C/min.
The temperature was then raised to 500°C at a linearly programmed rate of 10°C/min, and the catalyst was reduced for 12 h under hydrogen flow and then cooled to 40°C.
Then, the TPR of each sample was performed using 5% H2 in argon stream at a flow rate of 40 ml/min at atmospheric pressure using Micromeritics TPD-TPR 2900 analyzer (Norcross, GA, USA) equipped with a thermal conductivity detector (TCD), heating at a linearly programmed rate of 10°C/min up to 850°C.
Then the temperature-programmed reduction (TPR) of each sample was performed using 5% H2 in Ar stream at a flow rate of 40 ml/min at atmospheric pressure using Micrometrics TPD-TPR 2900 analyzer equipped with a thermal conductivity detector (TCD), heating at a linearly programmed rate of 10°C/min up to 850°C.
Then the TPR of each sample was performed using 5%% H2 in Ar stream at a flow rate of 40 ml/min at atmospheric pressure using Micrometrics TPD TPR 2900 analyzer equipped with a thermal conductivity detector (TCD), heating at a linearly programmed rate of 10 °C/min up to 850 °C.
For analyses using the DB-WAX column, the initial oven temperature was kept at 40°C for 4 min and then increased to 180°C at a programmed rate of 5°C min−1, followed by a rate of 10°C min−1 to 230°C.
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How did clients and occupational therapists in the lifestyle-oriented program rate the working relationship and were there any differences between these ratings?
The on-chip resistive heater employing a temperature programming rate of 26 °C/s produced a peak capacity of eight within a 1.5-s time window.
A full 33 factorial design was used to locate the optimum conditions for the temperature program, utilizing initial oven temperature, Ti, the programming rate for the first ramp, PR1, and the programming rate for the second ramp, PR2 as independent variables.
The programming rate and hold times were the same for both columns.
6. School personnel actively participate in the IAQ program (rate participation by each group).
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