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Synthesis of ERW1041E was performed according to published procedures (Scheme 3) [9].
Azinesulfonamide analogs of aripiprazole 1 6 were prepared according to previously reported procedures (Scheme 1) [5, 6].
α-[2(Trimethylsilyl)ethoxy]-2 N-[2- trimethylsilyl -ethoxycarbonyl]folic acid (7) was prepared accordiN-[2- trimethylsilyl -ethoxycarbonyl]folic matched the reported physical coN-[2- trimethylsilyl -ethoxycarbonyl]folicd S2).
Similar(57)
It is called procedure scheme.
All the other compounds are synthesized according to the procedure (Scheme 2).
IThroughporthis to poinewout that even if this procedureconcerned with purely Lagrangian schemes, the theorobustnessed is of fundamental importance for any methighlyelyimproved purely Landangian step, as ALE methenceor new-direct Euler schemes.
Open image in new window Fig. 3 Two-step FDE test procedure scheme: LS residuals (left) and KF innovations (right).
The kinetic experiment was carried out by changing the concentration of monomer, initiator, catalyst, temperature, etc., by adopting above stated polymerization procedure (Scheme 2).
The kinetic studies of polymerization were carried out with varying the content of monomer, initiator, catalyst and temperature by adopting the above procedure (Scheme 1).
The complexes 58 and 59 were synthesized with a similar procedure (Scheme 20) used for complexes 64/65 except that trimethylsilyl chloride is used instead of chloro cyclopenta-2,4-dienyl dimethylsilane for introduchloro cyclopenta-2,4-dienyl dimethylsilane
The SI-ATRP of styrene (St) from the BrA-SN macroinitiators was accomplished by the following procedure (Scheme 1): BrA-SN 0.5 g, the monomer (St) 15 mL, 215 mg (1.5 mmol) of CuBr, and 470 mg (3 mmol) of bpy were added into a dry round-bottom flask.
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