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The therein presented recovery algorithm exploits a priori knowledge on the structured nature of the signal.
The accuracy of the method was assessed by recovery experiments of Fe spiked that presented recovery of 103.28%.
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Method 3 presented recoveries that were higher than other methods and closer to 100%%.
Validation of the optimized method presented recoveries higher than 90% with RSD below 10%, showing good accuracy and precision.
After 3 months at − 20 °C, all compounds with the exception of temozolomide, vinorelbine, imatinib and erlotinib presented recoveries below 80%.
Method validation presented recoveries from 70.1% to 120.0% with RSD<20% and method limit of detection ranged from 0.3 to 7.5 µg kg−1, showing good accuracy and precision.
The quantitative method presented recoveries ranging from 73 to 116%, with precision (RSD) lower than 20%, for the 35 substances in the scope of the target method.
The validation results of the validation were satisfactory, since the method presented recoveries between 70% and 118%, with RSD lower than 19% for spike levels between 10 and 100 μg L−1.
The optimised method presented recoveries in EVOO between 91% and 115% for the target analytes (except vanillin with 65%) and a satisfactory precision with relative standard deviations (RSD%) lower than 8.4% for repeatability and reproducibility.
Coronary flow presented fast recovery, slow recovery, and plateau period after repeat coronary microsphere injection and remained reduced till 7 days after microsphere injection and returned to baseline level at 28 days after microsphere injection as evidenced by TFC.
Correction: October 14, 2003, Tuesday An article yesterday about the presidential campaign of Senator Joseph I. Lieberman referred incorrectly in some copies to the organization to which he presented a recovery plan for Iraq in October 2002.
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