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Preparative experiments led after alkylation to the formation of N-methyl-hydrazobenzene and N,N′-dimethylhydrazobenzene.
Preparative experiments using calorimeter, Mach probe and high-speed camera have been started at the end-mirror region and the heat flux density of the level in 1 10 MW m−2 was achieved in standard hot-ion mode plasma-confining experiments, which gives a clear prospect of generating the required heat flux density for divertor studies.
Similarly, in preparative experiments where mixing is considerably slower than in the stopped-flow chamber, the same proton-transfer chemistry can occur.
The most likely explanation, which was supported by DFT computations, was that at the temperature of the preparative experiments (∼100 K higher than the EPR study) the spiro-cyclization became reversible whereas the 6- ortho-process did not.
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A preparative experiment was carried out with initial concentration of the dye 500 µM and 0.11 M NaCl as a supporting electrolyte at a constant applied current density of 34.96 mAcm−2 and initial pH 3.9.
In a preparative experiment, NCC 1 (192.9 mg) was adsorbed on silica gel 60 (19.3 g).
In a preparative experiment, a solution of Mc-FCC-56 (31 μmol; containing about 30%% of its isomer, Mc-FCC-53) in aqueous citric acid (0.02 m) was stored for 159 h under an argon atmosphere in the dark at 15 °C.
Further studies of preparative electrolysis experiments by constant current electrolysis were carried out.
The electrocatalytic properties of the roughened TiO2 film electrode towards the electrocatalytic reduction of furfural to furfural alcohol were evaluated by CV and preparative electrolysis experiments.
Further studies of preparative electrolysis experiments by constant current electrolysis are carried out to confirm the high conversion to benzaldehyde, and the results are in good agreement with those from in situ FTIR investigations.
After 1y of in situ growth, 88 fragments of experimental set 1 (73.3%) and 48 (66.7%) preparative of experiment 2, developed colonies of different shapes.
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