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Since KLK5 is thought to be one of the most important enzymes involved in this process, we started a preparative attempt to identify KLK5 inhibitors in human stratum corneum.
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Though a number of preparative protocols have been attempted and introduced to control the shape of silver nanoparticles [16 20], analogous reports for AuNPs are comparatively few and are more recent.
Therefore, as we have extended the use of this modality for tolerance induction from mice to large animal models, we have attempted to design preparative regimens that avoid both of these complications.
Due to a relatively high cost of a preparative column packed with styrene divinylbenzene, an attempt was made to replace it with a traditional normal- or reverse-phase packing.
Based upon the proposed biogenesis of acortatarins [2], we envisaged the chemoselective Amadori rearrangement to get the furanoid amino sugars, but our attempts did not give acceptable preparative yields (see supporting information).
Having demonstrated the ability to successfully perform halide exchange on the pre-formed [GaCl(L)] complex on a preparative scale by using F−, radiofluorination was attempted.
Ceramic Preparative Methods.
Preparative and Mechanistic Aspects". 44.
Preparative and Mechanistic Aspects". 55.
Electrophoresis can also be used in a preparative mode.
H.R., W.S., M.d.V. and F.J.D. performed preparative biocatalysis.
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