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Powdered samples were pressed to form pellets and used for LIBS analysis.
For SEM, the powdered samples were used without any pretreatment or coating.
Further, the powdered samples were dried at 105 °C for 4 h.
Fine powdered samples were air-dried and stored at – 4 °C in polythene bags until use.
Powdered samples of the soil were pelletized and sieved to 0.074 mm.
Powdered samples were collected and kept in clean air-dried plastic bag for testing purpose.
The powdered samples were mounted on standard specimen stubs with double adhesive carbon tape.
The powdered samples are subjected to physico-chemical parameters as follows.
Different extracts were prepared by Soxhlet extraction with methanol of powdered samples of either leaves or fruit.
The crystal sturcture of the high temperature modifications have been determined be elastic neutron scattering experiments on powdered samples.
The powdered samples were scanned from 20 to 80 2θ at 1°/min with a scanning step of 0.0001°.
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