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Ca. 0.5 g of catalyst, diluted with equal amount of quartz grains, was positioned between two layers of quartz wool at the center of reactor.
In each catalytic run, about 1 g of the catalyst (crushed to 18/25 BSS sieve to eliminate mass transfer limitations) diluted with an equal amount of silica beads to maintain the isothermal conditions, was positioned between two layers of quartz wool at the centre of the reactor comprising 14 mm internal diameter and 300 mm length.
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