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A 16.5 mg mL−1 solution of diF-TES ADT in chlorobenzene was spin-coated at 104 rad s−1 (1000 RPM) for 80 s and placed under vacuum for 90 min to remove additional solvent.
The sample was then placed under vacuum to evaporate the remaining solvent.
The quartz tube is placed under vacuum and the furnace is heated up to a fixed temperature, around 1000°C.
The sample was placed under vacuum for 12 h, in order to evaporate the solvent remaining in the surface.
At the second and fourth week's interval, the samples were removed from the solution and placed under vacuum at room temperature and the mass loss was determined.
Finally, the remaining samples were oven-dried 30 60 minutes at 105°C, then transferred to a desiccator and placed under vacuum.
Similar(22)
Precooling can be accomplished by hydrocooling (immersion of the fruit in cold water) or vacuum cooling (moistening and then placing under vacuum in order to induce evaporative cooling).
An exception to this was the mineral oil, which did not remain in the coating layer after drying and placing under vacuum due to its volatile nature.
It was filled with 5 μm-filtered tap water, which had been degassed by placing under vacuum at <−635 mm Hg for at least 12 hours prior to each experiment.
A hot-pressed pellet of Cu1.97Ag0.03Se was placed under dynamic vacuum on an Anton-Paar DHS-1100 hot stage with an X-ray transparent graphite dome.
In order to investigate the influences of an ambient gas on the composition and the thickness of TiNi thin films, the films were placed under high vacuum (5 × 10-6 Torr) and in a 200-mTorr Ar gas.
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