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Three types of pit geometry are in evidence.
The influence of crystal packing is clearly demonstrated by several aspects of etch pit geometry.
Dislocations of different character have dissimilar strain fields and may give rise to variations in etch pit geometry.
The presented methodology is flexible, and can be adapted depending on a given mine's block sizes and pit geometry.
In addition, a study of the influence of the pit geometry on the fatigue life was carried out.
So far, much effort to fabricate pyramidal pit geometry was based on wet etching technique-induced large engineered architectures which limited their potential application [30, 31].
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Fig. 4 Energy decreasing during the evolution of pit geometries.
For the ellipsis geometry, the ratio should range from 1.4 to 1.8 with the composition and gas flow of the etching gases as CF4 (26 sccm)/CHF3 (5 sccm)/SF6 (40 sccm)/Ar (5 sccm)/O2 (5 sccm), whereas for the pyramidal pits geometry, the ratio should range from 2 to 2.5 with the composition and gas flow of the etching gases as CF4 (20 sccm)/SF6 (40 sccm)/Ar (5 sccm)/O2 (5 sccm), respectively.
However, shape and size of the CNT flowers were dependent on local geometry of the pit. Figure 2d is an SEM micrograph of typical CNT films on porous Si substrates (sample 4) showing honeycomb-like morphology.
The geometry of the pits depended on the face on which they occurred.
The three dimensional geometry of the etch pits was revealed using optical and interference microscopy as illustrated in Figure 3.
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