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The working curve with good linear correlation was established by using a phosphorus solution certified RM (SRM3139a) from NIST (Fig. 3b).
A phosphorus solution RM from NIST (SRM3139a) was applied as the external standard calibration, so as to guarantee the traceability for the quantification.
Fertilization was accomplished by the addition of 100 mL micronutrient solution (H3BO3, 7.5 mg; Na2MoO4·2H2O, 0.3 g; CoSO4·7H2O, 0.0045 mg) per pot and 200 mL of a phosphorus solution to provide 550 mg K2HPO4 per pot.
Fig. 3 HR-ICP-MS analysis results: a HR-ICP-MS spectrum of phosphorus in DNA (pStx2), b the standard curve for phosphorus analysis using phosphorus solution certified RM (SRM3139a).
Thus, main uncertainty sources were: first, the uncertainty of C s including the SD of 8 replicates, the uncertainty of the phosphorus solution RM and the uncertainty of the standard curve fitting; Second, the uncertainty of V s and V which came from the uncertainty of the pipettors and the volumetric flasks, and the volume change due to the temperature variation.
- Standard Phosphorus Solution: (100 m g P in 1 ml): Dissolve 438.7 mg of monobasic potassium phosphate, KH2PO4, in water in a 1000-ml volumetric flask, dilute to volume with water, and mix.
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The influences of pulse voltage on microstructure and phosphorus content, solution composition on discharge starting voltage and phosphorus content were studied.
Proper soaking of preforms at high temperature (1050 °C) eliminates iron-phosphide eutectic and brings entire phosphorus into solution in iron.
A novel calcium decorated sludge carbon (Ca-SC) was developed from dyeing industry wastewater treatment sludge by decorating calcium (Ca) to effectively adsorb phosphorus from solution.
Removal of total arsenic, iron and phosphorus from solution was enhanced within amended channels over unamended channels, with 7% of total As removed in amended channels vs. 3% in unamended channels.
The cathodic chamber is filled with a phosphorus buffer solution following the procedure described in [30].
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