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In this work, the hydration of Q phase-gypsum systems were investigated in terms of the kinetics, phases evolution and microstructure development.
The phases evolution mechanism in the HIP-processed Ti-43.5Al-6.5Nb-1.5Cr-0.5C/TiB2 parts can be divided into four steps: first of all, β phase transforms to γ and α phases, then, a small amount of new phases of TiB and TiC emerge by the diffusion of Ti and C atoms, subsequently, the β and α orderly transform to B2 and α2, lastly, the B2, α2, TiB2, TiB and TiC uniformly distribute in the γ matrix.
By combining high-resolution transmission electron microscopy and Rietveld analyses of X-ray diffraction patterns together with the local chemical data obtained by atom probe tomography, this research provides relevant information at the atomic scale about the mechanisms of crystallization and the subsequent phases evolution.
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The phase evolution was studied by X-ray diffractometer.
XRD was utilized in their work to observe changes in lattice parameters and phase evolution.
We can observe directly the phase evolution process of obtained TiO2 nanostructures with increased HCl concentrations.
Phase evolution was examined using an X-ray diffraction [XRD] diffractometer (X'Pert, PANalytical B.V., Almelo, The Netherlands).
This evidence strongly supported the stoichiometry phase evolution of the tungsten oxide.
The mechanism for the structure and phase evolution is investigated in detail.
These results demonstrated that phase evolution pathway and resulting powder properties were determined by feedstock powders.
After each processing stage, microstructural and phase evolution were monitored by SEM/EDS and XRD.
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