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In the wash-out system, the dispersed phase fraction was increased from zero continuously until phase inversion occurred; and in the batch case, concentration from 0.05 in steps of 0.1 volume phase fraction up to phase inversion were used.
A lost mold shape-forming process based on high-resolution microstereolithography technology was used to form the global pores, and conventional scaffold fabrication methods, such as salt leaching and phase inversion, were added to the molding process to generate local pores.
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New spectral evidence for phase inversion is presented.
Phase inversion was corroborated by transmission electron microscopy.
The phase inversion was observed at ηdghm = 0.05.
In PIT, phase inversion is driven by a temperature change without varying system composition.
The precursor fibres were removed from the external coagulant bath after the phase inversion was completed, and subsequently dried and straightened at room temperature.
Hence phase inversion was assumed to occur when the coalescence frequency exceeded that of breakup.
Blends were prepared at compositions where phase inversion was expected to occur according to model predictions.
No phase inversion was observed in ESBA with 60 wt% SBA.
The phase inversion was also found to shift towards lower EVA content under shear stress.
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