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Performed hardness test of the fractured crank pin showed that large HRC values were observed in central part of the pin only.
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The 24 h annealing performed during hardness measurements, up to 400 °C, induced thermally-activated processes in the thin films, which modify the critical load, hardness, and reduced elastic modulus of the thin film when measured at 23 °C.
Mechanical and microstructural characterization is performed by hardness testing and EBSD measurements.
Though the performed micro-hardness measurements clearly indicate surface decarburization effects and quantify the decrease in strength, they do not reveal the insufficient martensitic transformation during the thermal treatment of selected specimens (protocol 1).
Vickers hardness testing was performed to determine the hardness of the sintered structures.
Measurements of hardness were performed by the method of sclerometry (hardness under failure) and by load depth-sensing nanoindentation (hardness under eload depth-sensing deformationanoindentation
Microhardness was performed using Vickers hardness tester.
Measurement of hardness performed on pressed tablets has been also involved.
Microindentation experiments were performed to evaluate hardness and elastic modulus, which were found to decrease as the fluorine content increases.
Indentation studies were performed to analyze hardness, cracking behavior, and fracture toughness of bias varied pristine to re-heated specimens.
The surface scans of the hardness performed with this technique showed that anomalous regions can be identified that direct optical or scanning electron microscopy observation do not reveal.
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