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The peak integration range is typically 0.40 Hz.
ChemStation B.04.03 software (Agilent Technologies, Böblingen, Germany) was used for peak integration.
Black vertical lines indicate peak integration boundaries, and colored peaks represent the different transitions (i.e. peptide fragments) collected.
Plate cost includes LC/MS/MS plate preparation, plate run, peak integration and data processing/analysis/interpretation.
The preferred method is the terminal peak integration, with the same caveats as for monodisperse samples.
Two techniques for constructing calibration curves from the data, peak integration and partial least squares regression, were quantitatively evaluated.
For low numbers of entanglements, the terminal peak integration method requires a careful extrapolation at the high frequency side.
Purities of bicyclic polymers were estimated from SEC traces by Gaussian multiple peak fitting and subsequent peak integration.
Dashed lines indicate peak integration boundaries.
Shaded zones indicate peak integration boundaries.
Blue lines show the results of peak integration.
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