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The absorption band of PPHT: ZnO blend becomes stronger and the absorption peak ascribed to PPHT is shifted towards the longer wavelength region (red shift) upon thermal annealing.
They also exhibited a broadband ranging from 506 to 599 cm−1 which includes the 540 cm−1 peak ascribed to the ZnO 2LA mode [9].
The spectra of FTIR ATR adopted the appearance of an absorption peak ascribed to carbonyl group, and XPS showed reduced F / C and increased O / C.
Notably, the peak of 002 plane moves to a much higher angle (23.5°) and the peak ascribed to 10 plane appeared after the carbonization treatment, suggesting VFs were graphitized.
The presented data demonstrate the correlation between the presence and intensity of the Raman peak ascribed to the labelling molecule and the production of COOH groups on the nanotube walls.
Only single peak ascribed to the glass-to-rubber transition is detected in the tensile loss modulus curve for PMMA/PVB/LiCF3SO3 (70/30/20), although there are distinct double peaks for PMMA/PVB (70/30).
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XRD and Raman measurements performed on the doped powders showed only peaks ascribed to pure anatase.
The XRD peaks ascribed to the Mg−Al oxide disappeared in 10 min, and peaks ascribed to hydrotalcite (JCPDS card 22-700), a naturally occurring hydroxycarbonate of magnesium and aluminum (Mg6Al2(OH)16CO3·4H2O) with a layered double hydroxide structure, increased with time.
Main diffraction peaks ascribed to the (112), (220), and (312) planes of CZTS are easily identified all the three patterns.
FTIR spectra of TiO2@DTMBi NSs clearly show the characteristic absorption peaks ascribed to DTM ranging from 1,230 to 1,650 cm-1 (Figure 4a (spectrum 1), indicated by the arrows).
FTIR spectra of RT NPs clearly show the characteristic absorption peaks ascribed to TPB at 612, 707, 735, 1,014, and 1,427 cm−1 (Figure 2d, indicated by black arrows) and the typical absorption peaks ascribed to RAC at 1,092, 1,479, and 1,578 cm−1 (Figure 2d, indicated by blank arrows).
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