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(d) Expected pattern of the nanoparticle array.
It was confirmed that the self-agglomerating pattern of the nanoparticle in the polymer melts plays a key role in directing the morphology evolution of the immiscible polymer blend: unlike the self-agglomeration of carbon black to form three-dimensionally continuous network structure, the TiO2 nanoparticles tend to form separate clusters in the PA6 phase.
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d X-ray diffraction pattern of the nanoparticles showing peaks typical for gold.
Open image in new window Figure 3 X-ray diffraction pattern of the nanoparticles.
The SAED pattern of the nanoparticles, as shown in Fig. 1c, exhibits electron diffraction spots in a ring pattern, indicating the formation of NiO nanoparticles which are polycrystalline.
X-ray powder diffraction (PXRD) pattern of the nanoparticles is recorded on a Panalytical Empyran with Cu Kα radiation in the range 2θ = 0° 140°.
The XRD pattern of the nanoparticles formed by 1064 nm wavelength laser beam in deionized water and methanol at room temperature reveals that they are crystalline and possess the hexagonal Wurtzite structure [16].
Further support for the stability of the Pd nanocatalyst was provided by HAADF-STEM analysis, which showed that the recovered catalyst exhibited a similar nanostructure to that of the unused catalyst, without any observable change in either the size or dispersion pattern of the nanoparticles.
Figure 2 presents the XRD pattern of these nanoparticle thin films.
Figure 4B shows the SAED pattern of the CdS nanoparticles indicating that nanoparticles were crystalline in nature.
We found that compared to those of the nanoparticles of pure lithium silicates, the diffraction lines in the powder XRD patterns of the nanoparticles of Sb3+-doped lithium silicates shift to lower 2θ values.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com