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Fig. 1 XRD pattern for sample Run-15.

Figure 2b exhibits the OIM pattern for sample 2. The color distributions of the pattern were blue-green, green, and yellow-green, according the maps legend, the grain misorientation angles of Y2O3 were 5°~9°.

The results followed the same pattern for samples obtained after freezing and thawing.

Also looking at the last stage deformations, the pattern is regular for samples of lower strength materials, while it is of irregular pattern for samples with strength materials.

(b) The representative XRD patterns for sample S1 annealed at 200°C, 400°C, and 800°C.

X-ray patterns for sample 1 of 26:13:0 grade demonstrate the presence of (NH4 2HPO4, NH4H2PO4, (NH4 2SO4, 2NH4NO3·(NH4)2SO4 and 3NH4NO3·(NH4)2SO4 and for the sample 2 the presence of NH4NO3, NH4H2PO4, 2NH4NO3·(NH4)2SO4 and 3NH4NO3·(NH4)2SO4.

Open image in new window Figure 2 Rietveld refined XRD patterns for sample S1 (CoFe 2 O 4 : citrate method) annealed at (a) 200°C, (b) 400°C, and (c) 800°C.

Open image in new window Figure 3 Rietveld refined XRD patterns for sample S2 (CoFe 2 O 4 : co-precipitation method) annealed at (a) 200°C, (b) 400°, and (c) 800°C.

Comparison of the diffraction patterns for sample (b) indicates that the 2D-hexagonal ordering has been retained after the binding of DA- APTES into mesopore channels of SBA-15.

An estimator that was a compound of three basic distance estimators was found to be robust across all spatial patterns for sample sizes of 25 or greater.

Figure 1 X-ray diffraction patterns for samples S700, S800, S900, and S1000.