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Sample Z6 has maximum particles in the range of 10 18 nm.
TEM showed the average size of the particles in the range of 28 41 nm.
TEM images of the samples confirm the nano-size of the particles in the range of 10 90 nm.
These images illustrate the uniform spherical morphology of the synthesized particles in the range of 40 to 50 nm.
The experiments used 95% pure commercial boron powder with particles in the range of 0.4 30 µm.
SEM images show some agglomeration among the particles and the average size of the particles in the range of 50 90 nm.
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The optimal operation condition for preparing CMC micro-particles in the range of this work is: the pressure of 200 bar, the temperature of 55 °C, with 500 μm nozzle and 1 cm spraying distance in the presence of deionized water as cosolvent.
High-speed visualization of the sand impact on the material surface demonstrated fragmentation of almost every sand particle in the range of velocities of 60 m/s and higher.
The guest particles had particle diameters in the range of 1 10 μm, and surfaces that were l-leucine enriched.
Consequently, nano-sized TiO2 particles with particle size in the range of 10 20 nm have been synthesized.
Formulation F4 showed nearly equal percentage of weight fraction of the particles in the ranges of 250 500 and 600 710 μm.
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