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Yield: 62%, orange solids.
Yield of 4: 58%, orange solids.
Purification of 7 was performed by recrystallization from THF. Yield of 7: 54%, orange solids.
The resulting material showed an interesting ability to complex copper(I), giving stable yellowish light orange solids and aqueous solutions.
The obtained thiosemicarbazones were yellow or orange solids, insoluble in water, but easily soluble in ethanol, methanol, benzene, dichloromethane, chloroform, ethyl acetate.
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The product was obtained as orange solid.
Orange solid (yield 76 %), Elemental anal.
c Normalized PL spectra at 0 V (black solid) and − 1.6 V (orange solid).
The orange solid was filtered, dried in air and recrystallised from CHCl3.
When the potential is set to − 1.6 V (orange solid), the PL shows considerable quenching.
The orange solid curve is the stacking velocity function used for NMO correction.
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