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We report the study of different aspects of the aerosol-assisted chemical vapour deposition (ACVD) method for the optimised synthesis of multi-wall carbon nanotubes (MWCNTs).
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The development of optimised syntheses of the required molecular scaffolds is described, in which reactions including Pd-catalysed aminoarylation and diplolar cycloadditions have been exploited as key steps.
This paper presents an optimised hydrothermal synthesis of HKUST-1 and an analysis of water stability of HKUST-1.
Here, we report an optimised two-step synthesis of annexin A5-diethylene triamine pentaacetic acid (DTPA) (anxA5-DTPA) for positron emission tomography (PET) and single-photon emission computed tomography (SPECT) imaging with a single purification step.
We detail an optimised solution phase synthesis employing a convergent assembly of peptide building blocks, giving access to the minigramicidines and a succinyl linked gA derivative on preparative scale.
The optimised method for the direct synthesis of maleimide-DTPA linker 4 from cyclic DTPA anhydride 1 and N- 2-aminoethyl) maleimide trifluoroacetate 2 preseN- 2-aminoethyles siN- 2-aminoethylesis using inexpensive reactants.
We then proceeded to develop an optimised method by attempting oligomer synthesis and broadening the monomer set.
Three factors were optimised: the ageing time of the synthesis gel, the crystallisation time and the crystallisation temperature.
This protocol describes our optimised protocol for high-level bacterial synthesis of soluble antibody scFv fragments, as either monomers or multimers, using the heat-inducible bacterial expression vector pPOW3.
The latter synthetic procedure was optimised by performing a number of syntheses varying the reaction solvent, catalytic complex and the temperature used.
Recent work on the synthesis of ZnO NPs was optimised to ensure relatively smaller sized particles were obtained.
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