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Urine samples were enzymatically de-conjugated with β-glucuronidase and then extracted by an optimal USAEME procedure for the measurement of total concentrations of target analytes.
Even with that complication, the fact that the linear relationship total area versus concentration is hold reinforces the applicability of BiFE for the determination of total concentrations of metal ions inside a wider concentration range than that initially expected.
The lowest proportions of EDTA extractable fractions of Ni and Co (up to 7 and 4% of total concentrations, respectively) are observed in soils derived from proper serpentinites devoid of primary minerals (e.g., olivine, pyroxene) and having non-pseudomorphic texture.
Results showed that a total of 68 volatile compounds were identified among which H2S (56.58–579.84 μg/m3) and NH3 (520–4460 μg/m3) were the notable odor components contributing to 4.47 10.92% and 83.91 93.94% of total concentrations, respectively.
A liquid chromatography tandem mass spectrometry (LC MS/MS) method for the determination of total concentrations of lopinavir in plasma was developed and validated, and an adaptation was also optimized and validated for the determination of unbound concentrations.
Sample weighing 0.5 g was digested within a mixture (1 3) of per chloric (HClO4) and nitric (HNO3) acids for the determination of total concentrations of macro- and micro-elements [potassium (K), calcium (Ca), magnesium (Mg), sodium (Na), copper (Cu), iron (Fe), manganese (Mn), and zinc (Zn)], using an atomic absorption spectrophotometer (AAS) (Miller 1998).
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Its victory this weekend, achieved with Getafe's one attempt on target all evening, was ground out of total concentration on containing Barcelona in midfield and defense.
In it he recalls his fixation with learning how to copy Lyon's Juninho Pernambucano, and the magical moment in which he finally understood what he had been doing wrong: "The best ideas come about in moments of total concentration … My own Eureka moment arrived when I was sat on the toilet.
For OLM assay, isoabsorptive method [19] was applied for determination of total concentration of OLM and HCT.
The order of total concentration of the organochlorine pesticides was Plot4 > Plot1 > Plot5 > Plot3 > Plot2.
The method permits also determination of total concentration of active sites on the catalyst surface.
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