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Anti-Vibrio activity of each collected peak was assessed using V. vulnificus as indicator.
Comparison of mass spectrum of each collected sample with that of each standard sample (bilobalide, ginkgolides, A, B and C) was conducted.
GC MS spectrum of each collected sample after TMS derivatization was identical with that of each standard sample (bilobalide, ginkgolides A, B and C).
Analysis of the TMS derivative of each collected sample was performed with a Shimadzu GC MS QP2010 (Shimadzu, Japan) equipped with a TC-5 capillary column (30 m, id: 0.24 mm).
A volume of 500 ml of each collected water sample filtered with Whatman 41 filter paper was taken in a clean weighed porcelain dish followed by addition of 4 gm of cellulose powder and evaporated on water bath.
Loss of methyl moiety from molecular ion [M CH3]+ of each collected sample also showed at m/z 455, 537, 625 and 713, respectively, which are identical with that of authentic bilobalide, ginkgolides A, B and C. The HPLC and GC MS spectra strongly indicate that bilobalide, ginkgolides A, B and C were produced in the callus derived from the leaves of G. biloba.
Similar(36)
Three research teams, of three scientists each collected the data.
The mean degradation ratio of three pieces of film collected each time was calculated from mean gray values of digital images containing each collected piece.
Its leaking and bleeding across sky and water is captured by hundreds of cameras, each collecting a piece of rainbow.
Each analysis was replicated three times using three different pieces of each sample collected at different times.
The training and the manual should in detail highlight the significance of each variable collected.
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