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1H-NMR of the product dissolved in d6-DMS was carried out by using NMR of Varian Oxford-300 (300 MHz) spectrometer.
b: 13C NMR of compound 10.
(b) 29Si CP-MAS NMR of the composite before aging.
(c) 29Si CP-MAS NMR of the composite after aging.
1H NMR of ATC (liquid state) and its solvates.
1H-NMR of 8 showed singlet at 2.3 ppm for CH3 group, while 1H NMR of 9 exhibited two signals at 1.9, 2.6 assigned to 2CH3 groups.
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1H-NMR of the synthesized compound 3. Figure S2.
Fig. 2 1H-NMR of TMSPM/VP copolymer.
13C-NMR of the synthesized compound 3. Table S1.
1H-NMR of 6 exhibited singlet at 2.0 ppm according to COCH3 group.1H-NMR of 7 revealed singlet at 9.4 ppm for NH group.
MAS-NMR of tetrahedral 27Al was the dealumination yardstick.
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