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In addition, the kinetic parameters related to the solid state decomposition of the poly-nanoparticles were calculated by non-isothermal methods based on multiple heating rates.
Pyrolysis of RL and SL was performed on a TG analyzer at multiple heating rates of 20, 60, 80, and 100 °C/min up to 720 °C to obtain the thermal behavior of lignin substrates.
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The kinetics parameters, such as the activation energy, E (kJ/mol) involved in the polymer-to-ceramic conversion, were investigated by thermogravimetry using a multiple heating rate kinetic method.
Multiple melting endotherms were observed even at high heating rates, e.g. 160 K min−1 and these have been attributed to the presence of two different distributions of lamella thickness and re-crystallisation (reorganisation) on heating.
Note that the ASTM method is often the only effective approach to analyze reactions with multiple exotherms because these peak temperatures at different heating rates are not significantly influenced by the baseline shift [47].
The multiple melting peaks of isothermally crystallized poly ether ether ketone) were investigated by fast-scanning chip calorimetry over a wide range of heating rates from 500 to 60,000 K s−1.
Multiple heating, ventilation and air conditioning systems are becoming commonplace.
Geo says it's working on enabling multiple heating zones in future iterations of its product.
TG measurements were also performed at different heating rates.
The heat intensity was controlled by the individual's experience, from a starting baseline of 32°C, multiple heat cycles occurred at constant rates (1°C/sec ascending and descending), and applied to the forehead area (V1) ipsilateral to the headache using a 16 mm thermal probe system (Pathway Model- MEDOC, Ramat Yishai, Israel).
The relationship and the numerical statistical errors of conversion rate between the experimental data and the calculated data by the multiple linear regression method at the heating rate of 10 °C/min are shown in Fig. 3 and Table 4, respectively.
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