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Depending on the specific construct, this can improve the summed multiple coherence at frequencies where the response magnitude is low.
This paper presents a novel scheme to enhance the sensitivity of MQMAS using signals from multiple coherence transfer pathways.
The unsteady force measurement setup and calibration procedure were designed to minimize the effect of system resonances, and contamination from facility vibration was reduced using a multiple coherence noise removal technique.
In contrast, the combined use of stochastic estimation and IMBIC provides with accurate estimation results even with large friction: the multiple coherence functions are larger than 0.9 throughout the frequency range of interest and the estimated magnitudes and phases are well matched with that of a real human arm.
Additionally, the multiple coherence functions for each output approached 1.0 between ∼2 10 Hz. (Figure 7B).
Next, multiple coherence was used to determine the range of frequencies for which the linear transfer functions were appropriate [25].
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The results showed good quality in the reciprocities, and the multiple coherences in each degree of freedom were close to one in the frequency range of 25 500 Hz.
The structure of this isolated compound was determined by a combination of spectroscopic analyses, including IR, H and C NMR, hydrogen-hydrogen correlation spectroscopy (H-H COSY), heteronuclear multiple quantum coherence (HMQC), heteronuclear multiple bond coherence (HMBC), mass spectroscopic data, and chemical methods.
DOI: http://dx.doi.org/10.7554/eLife.03941.018 The H and C resonances of the isolated tetrasaccharide product were assigned by using heteronuclear multiple quantum coherence (HMQC), heteronuclear 2-bond correlation (H2BC), and heteronuclear multiple bond coherence (HMBC) spectra.
The structure of compound 2a was identified by 2D NMR including heteronuclear multiple-quantum coherence (HMQC), heteronuclear multiple-bond correlation (HMBC) and H H correlation spectrometry (H H COSY) spectra.
The 1H NMR spectra of ADP-1a, ADP-1b, ADP-2, ADP-3a, and ADP-3b were recorded, 13C NMR spectra, the 2D NMR spectra including heteronuclear multiple-quantum coherence (HMQC) and heteronuclear multiple bond correlation (HMBC) of ADP-1a and ADP-2 were recorded.
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