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The time for developing 50% of the total crystallinity (t1/2) was used to monitor the crystallization kinetics.
Turbidity measurements were used to monitor the crystallization process and to determine the polymer solubility as a function of temperature and pressure.
X-ray diffraction was used to monitor the crystallization process in the films during annealing, which indicated that the YSZ films started to crystallize at 300 400 °C and became fully crystalline with a cubic structure at temperature ≥ 600 °C.
To monitor the crystallization during freeze-drying, a Raman probe was placed just above the sample in the freeze-dryer.
Since these peaks can be clearly distinguished from each other, it is possible to use in-line Raman spectroscopy to monitor the crystallization of the individual components.
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Monitoring the crystallization process yields insight into the moment and length of the crystallization of the different components, while varying the process conditions reveals which factors influence the model drug crystal size and therefore the dissolution rate.
We have monitored the homogeneous crystallization of TiO2 phases from aqueous TiCl4 solutions at 100 °C using both time-resolved small-angle X-ray scattering (TR-SAXS) and time-resolved wide-angle X-ray scattering (TR-WAXS).
The time resolution of the in situ monitoring of the crystallization is dictated by the time required to record an individual NMR spectrum of adequate quality to identify and distinguish the different solid forms present during the evolution of the system.
The crystallization kinetics were estimated by monitoring the changes in the absolute value of complex viscosity during crystallization.
But who monitors the monitors?
The copolymer was quenched from the melt to a range of crystallization temperatures between 289 K and 316 K and the crystallization monitored by observation of the increase in radius of spherulites (microscopy) or the enthalpy of fusion (calorimetry) as a function of time.
More suggestions(15)
monitor the result
tracing the crystallization
screening the crystallization
control the crystallization
monitor the soil
monitor the election
monitor the reaction
monitor the calorie
monitor the download
monitor the land
monitor the trap
monitor the situation
monitor the sting
monitor the temperature
monitor the patient
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