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Cryogenic high-vacuum transfer into and out of the FIB/SEM was performed via a Quorum PT2010 cryo-preparation station using the modified specimen transfer shuttle device shown in Fig. 1e.
Performance of the devised cyclic test setup and modified specimen is scrutinised and remedial measures are discussed for the potential issues that may affect the functionality of the proposed testing method.
The new procedure used in this study has been verified by the measuring of fracture toughness of Al alloy, using both the modified specimen, as designed here, and the standard one.
Aluminization and nitridation increase the hardness from HV110 120 for the original α-Fe(Al) to HV1200 1500 for the modified specimen, which consists of an α-Fe(Al) matrix with γ′-Fe4N and rocksalt AlN.
Compared with the control, the mechanical properties and fire performance of BPF-specimen were improved obviously, and the more the resin retain, the better the properties of the modified specimen.
The ZnO modified specimen with 0.2 wt.% H2O2 in the electrolyte showed the highest crystallinity and performed 11.5 times enhancement in the photocurrent density when comparing to the H2O2-free one.
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The non-modified HA/PEEK composites display the same trend as the modified specimens with lower tensile strength and consist of sharp points.
Nevertheless a visible reduction occurred on the drying shrinkage values of FA modifying specimens more than cement specimens and GBFS modified specimens.
DSC and TGA tests were conducted to examine the thermal performance of the nanoclay modified specimens.
Even in the modified specimens, the orientation of the chain axis is maintained parallel to the draw direction.
As a matter of fact, there is negligible increase in the thickness of the specimens, less than 1%, but there is noticeable out-plane mechanical properties increase of the modified specimens.
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