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The mass spectrometer was operated in EI mode at an ionization voltage of 1047 V.
Injection was performed in a splitless mode at an injection temperature of 280°C.
The scanning was performed under a non-contact mode at an ambient condition.
Imaging was done in the high vacuum mode at an accelerating voltage of 20 kV, using secondary electrons.
Imaging was done in a high vacuum mode at an accelerating voltage of 20 kV, using secondary electrons.
The samples were analysed in splitless mode at an injection temperature of 250 °C and detector temperature 280 °C.
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