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The mobile phase was degassed by sonication prior to use.
The mobile phase was 0.05% trifluoroacetic acid in water.
The mobile phase was pumped at a flow rate of 1.8 ml/min.
The flow rate of mobile phase was set at 0.6 mL min−1.
The mobile phase was 30% methanol containing 0.05% TFA (LC-MS grade).
The mobile phase was 10 mM H3PO4-methanol (45:55, v/v).
The mobile phase was purchased from Eicom and delivered at a rate of 0.33 mL/min.
The mobile phase was composed of (A) water with 0.1% formic acid and (B) acetonitrile.
The mobile phase was composed of pet.
The mobile phase was acetonitrile (65%).
The mobile phase was 4.5 mM sulfuric acid.
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