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A bench-scale fluidised bed (105 × 200 mm) was operated for obtaining the gas temperature profiles.
An atmospheric-pressure bubbling fluidized bed reactor (BFBR) of diameter 100 mm was operated cyclically and batchwise, alternating between reforming/carbonation conditions and higher-temperature calcination conditions to regenerate the sorbent.
A SUPELCO C18 column (cat# 504955; 5μm, 150 mm x 4.6 mm) was operated at 25°C with a 0.8 mL/min mobile phase flow rate.
A Gemini-NX C18 column (150 × 21.2 mm, 5-μm particle size, 110-Å pore size; Phenomenex, Aschaffenburg, Germany) protected by a Gemini C18 pre-column (15 × 21.2 mm) was operated at a flow rate of 16 ml/min using gradient elution.
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Two specially designed VFSF, a roughing filter (RF) packed with expanded clay material (grain size: 3 6 mm) and a polishing filter (PF) with zeolite material (grain size: 0 5 mm) were operated in both single-stage and two-stage configuration.
All 5 patients with major displaced fractures (> 10 mm) were operated and 4 had good to excellent results (Table 1), although 1 patient (no.
The plasma torch, which was 20 mm long, was operated at room temperature (22°C).
The bed had a height of 50 mm and was operated at different air flow rates.
The transducer had dimensions of 2.5 × 7.5 mm2, it was cylindrically focused at 10 mm and it was operated at a center frequency of 11 MHz.
The Ultrasphere IP column (4.6 × 250 mm, Beckman, Brea) was operated at 25°C at 1.0 ml/min (0.5 ml/min of each pump).
The HPLC apparatus was a Gilson System equipped with a 234 Auto-sampler, a UV/VIS-155 detector and a 321 HPLC Pump (Gilson, U.S.A .. Luna C18 reversed-phase column with 5- μ particles and 4.60 × 250 mm (Phenomenex, USA) was operated.
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