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A typical procedure is described as follows (using BUDA as an example): BUDA (2.0 mmol, 0.99 g), 3,6-dioxa-1,8-octanedithiol (2.0 mmol, 0.38 g), AIBN (0.06 mmol, 10 mg), and THF (2 mL) were charged into a 10 mL flask, purged with nitrogen for 10 min, and reacted at 70 °C for 12 h.
3-Methyl-2-phenethylpyridine (5): 23-Methyl-2- phenylethynyl pyridinene 3-Methyl-2- phenylethynyl pyridineylamine 3-Methyl-2- phenylethynyl pyridine % palladium on carbon (30 mg), and EtOH (30 mL) were charged in a round-bottomed flask.
2-(Benzyloxy -3-methylpyridine (6): 24 2-Chloro-3-methylpyridine (128 mg, 1 mmol, 1 equiv)., phenylmethanol (140 mg, 1.3 mmol, 1.3 equiv)., KO tBenzyloxy -3-methylpyridine)., and dioxane (5 mL) were charged in a round-Benzyloxy -3-methylpyridine
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A solution of anisole (1 mL, 9.2 mmol) in cis/ trans-decahydronaphthalene (20 mL) was charged into the reactor.
Then 1-pentanol (14.8 mmol, 1.62 ml, 2 equivalent), cyclopentylmethylether (solvent, 30 ml), 3 Å molecular sieves (800 mg) were charged under an argon stream.
For BOD tests, five 300 mL BOD bottles were charged with the wastewater with the same dilutions.
The supernatants were loaded on a Hitrap Chelating HP 5 ml column, which were charged with chelated Ni2+ and equilibrated with Buffer A for the first step of purification.
A mixture of 0.30 g FC-POP, 1.50 g paraformaldehyde, 9.0 mL acetic acid, 4.5 mL phosphoric acid and 30.0 mL concentrated hydrochloric acid were charged in a flask, by following a well-known method (Lu et al. 2012).
In a typical run, 1.8 g of NIPAM, 0.2 g of MBA, the crosslinker monomer, and 90.0 mL of deionized water were charged into a glass bottle of 120-mL capacity, which was located into a thermostat shaker at room temperature and shaken until the complete dissolution of the monomers, followed by N2 purge of the reaction system for 5 min and addition of 0.04 g of APS dissolved in 8 mL of water.
Aliquots of Pd (II) solution (0.2 mL, 8.07 mM each) were charged to the leaf extract solutions of C. cainito to prepare a series of stabilized PdNPs where concentration of the leaf extract varied from 80 to 400 mg L−1 and the concentration of Pd (II) was fixed at 1.614 mM.
For a typical reaction, 30 mg PANI CNT‚ 110 mg FeCl3-6H2O and 110 mg Co(NO3 2-6H2O NO3 2-6H2Oed into 50 mL EG, suspension agitating weredone by bath ultrasonicharged0 minto
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