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(0.5 g) and hydrazine hydrate (1 ml) in ethanol (15 ml) was refluxed for 1 h.
A solution of 2 (1 mmol) in DMF (10 mL) was refluxed with Conc.
A solution of each new compound (1 mg) in 0.5 N HCl (3 ml) was refluxed for 4 h.
The mixture of 9 (0.20 g, 0.31 mmol) and triethylphosphate (10 ml) was refluxed for 24 h.
A mixture of 9 (1.48 g, 5.48 mol) and benzylidenemalononitrile (0.54 g, 6 mol) in piperidene (10 mL) was refluxed for 3 h.
A mixture of compound 6 (0.95 g, 4.87 mmol) and hydrazine hydrate (5.0 mmol) in ethanol (4 mL) was refluxed for 6 h.
Similar(12)
Compound 9 (0.3 g, 1.1 mmole), absolute ethanol (50 ml) and thioglycolic acid (2 ml) were refluxed 6 hrs.
Compound 2 (2.36 g, 0.01 mol) and hydrazine hydrate (0.9 mL, 0.02 mol) in ethanol (20 mL) were refluxed for about 5 h on oil bath.
Intermediates 1 (1.25 mmol), aromatic aldehyde (1.25 mmol), and piperidine (0.10 mmol) in acetonitrile (5 mL) were refluxed with stirring for 8 h.
p-Acetoxybenzoic acid 3 (5 g, 27.6 mmol) and thionyl chloride (25 ml) were refluxed for 1 h (till complete dissolution of the starting material).
An aqueous solution of HAuCl4 (100 mL, 1 mM) was refluxed for 5 10 min, and a warm (50 60 °C) aqueous solution of sodium citrate (10 mL, 38.8 mM) was added quickly [3].
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