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In a Florence flask, 2.5 ml of titanium isopropoxide and 119 ml of ethanol were mixed.
A 0.7 mL of titanium(IV) n-butoxide was added to a mixture of hydrochloric acid and deionized water.
The mixture was then stirred for 15 min followed by the addition of 0.5 mL of titanium butoxide.
Then, 0.4 mL of titanium butoxide was added and stirred at room temperature until the solution became clear.
The matrix sol was prepared by mixing 0.695 ml of titanium (IV) isopropoxide with 15 ml of isoproponal at room temperature and stirred for half an hour.
TiO2 solution was prepared by adding 2 mL of titanium (IV) isopropoxide in 200 mL of deionized water under continuous magnetic stirring at room temperature.
Similar(39)
First, 1 mL (3.4 mmol) of titanium(IV) isopropoxide was quickly added to 0.38 mL of HCl, with vigorous stirring in a 20 mL vial.
First, 0.90 mL (3 mmol) of titanium(IV) isopropoxide was added to 0.74 mL (3 mmol) of niobium V) ethoxide in an inert atmosphere glovebox to give a mixed alkoxide precursor.
Two different titanium particle sizes were used: 64 mL of large titanium particles (diameter, 3.2 4.0 mm) to fill larger spaces in mostly the proximal and distal areas of the Sawbones® femurs and 18 mL of the smaller titanium particles (diameter, 2.8 3.2 mm) to create the graft layer in the middle part of the reconstruction.
The resulting supernatant was then mixed with 1 mL of 0.1% titanium chloride in 20% (v/v) H2SO4 and centrifuged at 6000 g for 15 min.
The target sample container is a 30 ml cylinder constructed of titanium alloy, with walls thick enough to withstand these temperature and pressure conditions without distortion, fitted with a specially shaped front window, thin enough to allow backward muons to penetrate and stop completely in the sample volume without reaching the end of the cell.
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