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The carbon oxides, oxygen and water fluxes arising from the combustion of the carbonaceous deposits in a 5% O2/He mixture, were continuously monitored.
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The mixture was continuously stirred at 200 rpm.
The mixture was continuously stirred until a thick white gel was formed.
Then, the mixture was continuously stirred with a magnetic bar, at room temperature for 1 h.
Each mixture was continuously homogenized by means of a magnetic stirrer (250 rpm).
Deionized water was then added dropwise and the mixture was continuously stirred for 3 h.
The mixture was continuously stirred for another 24 h under the formation of a white solid.
The mixture was continuously stirred at 20 °C for 30 min. The solid product then was isolated by filtering with suction.
The reaction mixture was continuously purged with nitrogen gas to displace the air of the system avoiding the oxidation.
The whole mixture was continuously stirred and heated until it turned into a burgundy and clear solution.
The mixture was continuously stirred for another 24 h under the formation of a suspension of a white solid.
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