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The mixture was further incubated for overnight.
The reaction mixture was further stirred for 24 h.
The reaction mixture was further stirred at 0 °C for 30 min.
Reaction mixture was further stirred at rt for 2.5 h until completion as per TLC.
The mixture was further mixed through grinding to obtain silicone composites with different CuNW loading.
The mixture was further stirred for 30 min, maintaining the temperature at 0 10 °C.
Then, the mixture was further diluted using approximately 300-mL DI water.
Oleic acid was then added to the diethylene glycol solution, and the mixture was further stirred for 10 20 min.
The mixture was further washed several times with EtOH by centrifugation (10 min at 30 k rpm).
Under a blanket of nitrogen, the mixture was further heated to reflux (300°C) for 30 min.
The mixture was further heated at 160 °C for 8 h with gentle stirring to insure the reaction homogeneous.
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