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Water was added and the mixture was extracted with DCM.
Thirty milliliters H2O was added and the mixture was extracted three times with 5 mL CHCl3.
The resulting mixture was extracted with 0.5 M HCl and the organic phase dried under reduced pressure.
Subsequently, the mixture was extracted twice with n-BuOH/6 M pyridinium acetate buffer, pH 4.2 (3:1, v/v).
The mixture was extracted and analyzed using the developed method.
Then the mixture was extracted with 200 mL dichloromethane.
The mixture was extracted with dichloromethane (3 × 4 mL).
The mixture was extracted with DCM (three times 100 mL).
Similar(3)
The reaction mixture was extracted with CHCl3 (3 × 5 mL).
The mixture was extracted with equal volume of EtOAc and concentrated under vacuum to give a crude extract.
The mixture was extracted twice with 2 ml of hexane/ethyl acetate (80 20).
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