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The mixture was degassed with N2 for 15 min, then placed in a 4 mm diameter cylindrical Teflon mold with a 3 mm central steel post.
The mixture was degassed for 10 min.
The mixture was degassed by vacuum/nitrogen purging for three cycles.
The reaction mixture was degassed under vacuum for 10 min at 150°C.
The mixture was degassed by three freeze-pump-thaw cycles with N2.
The mixture was degassed with vacuum pump (0.28 mbar) and kept at 160 °C.
Similar(26)
Typically, 1 mmol of copper iodide and 1 mmol of indium acetate are dissolved in 5 ml of 1-dodecanethiol and 1 ml of oleylamine, and the mixture is degassed under vacuum in a 50 ml flask at 100 °C for 30 min.
The mixtures were degassed and refluxed at 90 °C for 5 h until transparent solutions were formed.
Polymerization mixtures were degassed in an ultrasound bath and rinsed with nitrogen for 30 min.
The prepolymer mixtures were degassed and one part of the mixture was mixed with red fluorescent beads (0.2 µm diameter, FluoSpheres Crimson carboxylate-modified beads, Invitrogen) and subsequently applied on a previously silanized (1H, 1H′, 2H, 2H′-perfluorooctyl-trichlorosilane, Sigma) micro-structured silicon dioxide mold.
In a 50-mL three-neck flask equipped with a condenser, a mixture of CdO, stabilizing ligands (oleic acid (OA) or stearic acid (SA)), and the solvent (ODE or a mixture of ODE and oleylamine) was degassed in primary vacuum for 30 min and then heated under argon to the reaction temperature (250 or 300°C).
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