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The product mixture was analysed by chromatographic and spectroscopic methods.
The composition of oligomers present in the reaction mixture was analysed with MALDI ToF during the course of polycondensation.
Twenty per cent of the peptide mixture was analysed by nano-liquid chromatography tandem mass spectrometry using an LTQ Velos-Orbitrap MS (Thermo Scoupledic) coupled with an Ultimate RSLCnano-LC system (Dionex).
Five microlitres of each reaction mixture was analysed by liquid chromatography high-resolution mass spechromatography high-resolutionent systemass0%–60% acetonitrile/water with 0.1% formic acid over 40 min; flow rate 0.2 ml min−1) on the RP column (Thermo Acclaim 120, C18 2.1 × 150 mm).
An aliquot of 1 µl of this mixture was analysed by GC-MS.
The resulting mixture was analysed on a PSQ96MA pyrosequencer (Biotage).
Similar(36)
The incubation and digestion steps were carried out at least in duplicate and at least two separate samples of each peptide mixture were analysed by mass-spectrometry.
10 μl of the amplification mixture were analysed by electrophoresis in 1.5 agarose gel and visualized by UV light after ethidium bromide staining.
It is worth noting that a control where the enzymatic reaction mixture is analysed without incubation (yield for time zero), did not result in the generation of methyl ester.
In addition, capsules' distribution and their integrity inside the asphalt mixtures were analysed using X-ray computed tomography.
In this study, the contribution of the chemical composition of the filler to the consistency and stripping resistance of filler bitumen mixtures is analysed.
More suggestions(15)
mixture was evaluated
mixture was explored
mixture was investigated
mixture was examined
mixture was characterized
solution was analysed
mixture was calculated
mixture was scrutinized
melt was analysed
mixture was discussed
mixture was centrifuged
mixture was injected
mixture was poured
mixture was degassed
mixture was prepared
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