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The mixture was allowed to react overnight.
The mixture was allowed to react at 30°C.
The mixture was allowed to react for another hour.
The mixture was allowed to react for 24 h.
The mixture was allowed to stand for 2 h.
The resulting mixture was allowed to evaporate in fume hood.
At an RPM of 200 for 10 h, the mixture was allowed for blending.
The mixture was allowed to stand in the dark for overnight.
The resulting mixture was allowed to stir at room temperature for 8 h.
After the addition of Grignard reagent, the mixture was allowed to warm up to rt.
The mixture was allowed to stir for several minutes at 5 10°C.
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