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Minor elements are in ppm. Figure 4 Variation diagrams.
2.44 2.06 3.63 10.89 6.02 4.29 8 6 6 Major and minor elements are given in mass percentages and expressed as oxides; trace elements are given in parts per million.
Based on the signature spectrum, the main elements present in the paint are Mn, Fe, Co, Zn and Pb, and minor elements are S, Ca, Ba/Ti, Sr and Zr.
Similar(57)
The relative standard deviation of the major and minor elements was 1% and less than 2%, respectively.
Some minor elements were also detected, such as Mg, Na, Si, etc. Figure 2 XRD patterns of calcined fish bones compared with commercial stoichiometric HA (JCPDS 1993).
The major elements were determined using a ThermoFisher IRIS Advantage inductively coupled plasma optical emission spectroscope; minor elements were measured using a ThermoFisher VG-X7 inductively coupled plasma mass spectrometer.
Major and minor elements were also analysed by LA-ICP-MS and were in line with the results obtained by EPMA (variation for silica of 2%, sodium 5.5%, potassium and calcium oxides 6%, magnesia 8%, alumina 10%, manganese 12% and iron oxides 15%).
Determining of major and minor elements was based on a two step method.
The chemical composition of the used substrate is presented in Tables 2 and 3. Determination of major and minor elements was achieved according to Standard EN 15290 and Standard EN 15297.
The two dominant elements belong to the scorpaenid and the cottid-hexagrammid lines, whereas the third, and minor, element is the anoplopomatid line.
Considering the severe degree of internal oxidation, decarburization and consumption of minor alloy elements are proposed to be responsible for this ferrite band.
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