Sentence examples for min the solvent from inspiring English sources

After 30 min, the solvent was evaporated in vacuo.

After 2.5 min, the solvent was removed under reduced pressure, and the reactor temperature was increased to 160°C.

After 30 min, the solvent was evaporated and the crude product was purified using preparative RP-HPLC (isocratic eluent: 18% B).

After 5 min, the solvent evaporated and the slides were removed from the chamber to allow water evaporation under ambient conditions.

During the first 7 min the solvent composition was kept at 100% "A" followed by a linear gradient over 3 min to 80% "B" and re-equilibration to the initial conditions.

After centrifugation at 5000 × g for 5 min, the solvent phase was recovered.

After 10 min, the solvents were evaporated in vacuo at low temperature and traces of TFA were removed by co-evaporation with EA (3 × 10 mL).

After 25 min the solvents were evaporated under reduced pressure and the crude product was purified by column chromatography on SiO2 (0–2 % CH3OH in dichloromethane v/v) to yield G3 as a red foam (4.05 g, 5.08 mmol, 85%%).

Solvent programming was isocratic 0% B for 2 min followed by 5% at 5 min, then linear gradient up to 100% B at 10 min and 100% B isocratic until 12 min. The solvent composition was returned to initial conditions at 12.1 min and recalibrated to 14 min. Flow rate was 0.3 ml/min.

Solvent programming started at 50% B with a linear gradient up to 95% B at 10 min, and 95% B isocratic until 12 min. The solvent composition was returned to initial conditions at 12.1 min and recalibrated to 15 min. Flow rate was 0.4 ml/min.

The mobile phase consisted of 0.1% formic acid (FA) in water (A) and 0.1% FA in acetonitrile (B) using a gradient program of 25-40% (B) in 0 4 min, 40-66% in 4 23 min. The solvent flow rate was 0.35 mL/min, the column temperature was set to 40°C and the detection wavelength was 258 nm.