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After 20 min of reaction, the ammonium generated was measured by Nessler's reagent as described above.
From77Se NMR integrated peaks, we calculated an average of 36% conversion of TnBPSe to H2Se after 15 min of reaction.
Under such conditions 86% removal of 2,5-DHBA was attained after 15 min of reaction.
The response function was the %TOC removal after 15 and 60 min of reaction.
The response analyzed is conversion of DBT at 15 min of reaction time.
The increase in surface area happened mostly in the first 10 min of reaction.
Factorial experimental design was used to assign each variable's weight in TOC removal after 30 min of reaction.
Factorial experimental design allowed to assign the weight of each variable in the TOC removal after 15 min of reaction.
The temperature, pH and concentration of free phosphate were monitored during the first 80 min of reaction.
However, after 300 min of reaction time, the mineralization increased to 87%, and the initial toxicity was reduced by 70%.
A very similar removal profile in the first 2 min of reaction was observed for both systems with a high degree of degradation (close to 90%).
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