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The milled samples of olive roots, stems, and leaves were characterized by Fourier transform infrared (FTIR) spectroscopy.
Hammer milled samples of as-received straw and dried treated residues were conditioned in the laboratory atmosphere to ambient moisture content, or were saturated with measured amounts of distilled water, followed by overnight equilibration.
Wheat straw was collected as raw material and a representative sample was made by mixing 16 different freeze dried and milled samples of wheat straw in the same ratio.
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According to the present research, it is worth noting that for the preparation of amorphous alloys from different kinds of metal using ball milling, it is not precise to consider the diffused halo peak appearing in the XRD pattern of milled samples as amorphous phase without the careful investigation of the microstructure.
The DSC curves of milled samples exhibit a strong broadening and a low-temperature shift of the Pb crystal liquid transition peak.
The X-ray diffraction (XRD) profiles of the milled samples do not show any significant modification of the ceria zirconia structure and all samples can be indexed in a fluorite cubic cell (see Figure S2 and Table S1 in the Supporting Information).
Open image in new window Figure 5 Williamson-Hall plot of milled samples.
As shown in Figure 4, all milled samples showed no presence of asiaticoside, and we believe that asiaticoside have been hydrolyzed to asiatic acid during the milling process.
A 2 4-1) factorial screening design was implemented to identify the spiral jet-milling process variables that significantly affect the particle size distribution of milled samples.
A further size reduction of milled samples was carried out prior to powder-type WAXD measurements, to 0.5 mm mesh size, using a laboratory hammer mill (Perten Gmbh).
For analysis of the other elements, milled samples were digested with a mixture of HNO3 and HClO4 at 200 °C with reflux cooling.
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