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Vessels content were mixed and kept at room temperature for 12 h, then the vessels were introduced in the microwave digestion system and digested using a four-step digestion program: (1) 5 min at 280 W, (2) 5 min at 700 W, (3) 10 min at 1,050 W, (4) 1 min at 0 W.
The obtained infusions were filtered, evaporated to approximately 10 mL on a hot plate, then 1 mL of HNO3 was added and the samples were digested in the microwave digestion system using the same digestion program as for solid samples.
Samples were digested in a Milestone EthosEZ microwave digestion system (Shelton, CT, USA) with a 120 °C temperature ramp for 30 min (600 W) and a 120 °C hold for 30 min (400 W), followed by a 45 min exhaust cycle.
Samples for metal analyses were digested with concentrated HNO3 in a microwave digestion system.
Each dried sample was weighed and digested with 11 N HNO3 at 200°C using a microwave digestion system (MDS Ethos1, Milestone, Italy).
A microwave digestion system was used to ensure continuous digestion.
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The microwave closed digestion system (Milestone, Start D) was used for the mineralization process.
The microwave closed digestion system (MDS 2000, CEM Corporation, North Caroline, USA) was used for the mineralization process.
The ca. 400 mg of grab-sampled and homogenized soil was transferred to a pressure liner from an Anton Paar Microwave oven digestion system together with 3 mL analytical grade concentrated HNO3 and 3 mL analytical grade concentrated HCl.
In order to determine the elements from the polymeric matrix, acid digestion was performed with a microwave-assisted digestion system (Speedwave four with DAK-100/4 PTFE closed vessels; Berghof, Eningen, Germany).
Wheat leaves and roots were digested with HNO3 by microwave digestion.
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