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Transmission electron microscopy and atom-probe tomography were used to characterize on a near-atomic scale the microstructure and oxide and carbide phases that form during thermo-mechanical treatments of a model oxide dispersion strengthened Fe 12 wt.% Cr 0.4 wt.% Y2O3 alloy.
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This chapter begins by explaining high-temperature corrosion thermodynamics, the Pilling-Bedworth ratio, electrochemical oxidation processes, oxide layer formation, microstructure, and oxidation kinetics.
The microstructure and thickness of oxide scale layer of stainless steels were obtained and two or three oxide layers can be found.
The oxidation behaviours of the alloys at 1150 °C were studied and compared in terms of oxide spallation, oxide microstructure and growth, residual stress in the α-Al2O3 scale and oxide/alloy interface morphology.
The oxidation kinetics, morphology and microstructure of the oxide scale and the microstructure of the bulk of the oxidised alloy were investigated.
SEM images of the film showed that the resulting surface exhibits different flower-shaped wurtzite zinc oxide microstructure and porous Zn Al LDH.
The microstructure and texture evolution of oxide dispersion strengthened ferritic steel during stepwise uniaxial tensile deformation were observed by high-resolution electron backscattered diffraction with a newly designed deformation device.
The microstructure and composition of the oxide films were analyzed by Scanning Electron Microscope (SEM), X-ray Photoelectron Spectroscope (XPS) and X-ray Diffraction (XRD).
The differences in the oxidation rate of both Ni crystal faces are interpreted by the changes in oxide microstructure and texture, in terms of the type and density of grain boundaries.
The relation between the multi-layered, nano-sized oxide microstructure and the colour is experimentally determined and translated into an optical model that is able to predict the colour as a function of microstructural variations.
Electronic property, microstructure and chemical composition of oxide films formed on Alloy 600 in high temperature water with various dissolved hydrogen (DH) levels that allow the Ni/NiO phase transition to occur were studied by employing electrochemical and exposure experiments.
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