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Spherical and compacted microspheres with average diameters of 100 600 μm have been prepared, and their release behavior in distilled water containing 1.2% (w/v) of polysorbate-80 can be controlled by the ratio of polymer/Areosil200 in the microspheres.

Monodisperse PS particles 1.05 μm in diameter were initially fabricated via dispersion polymerization, and PS/PEDOT microspheres with average diameters of approximately 1.07 μm were prepared by a swelling-diffusion-interfacial polymerization process.

The results showed that Ag0 particles were loaded to the gelatin microspheres with average diameter of 4.46 μm and Ag/GMSs distributed uniformly on the pore walls of PT and MPT.

The results revealed that microspheres with average diameter of 700 nm were formed by self-assembly of tiny TiO2 nanoparticles during the reaction at 25 °C, whereas spherical aggregation of nanofibres was detected in powders produced at 80 °C.

For example, microspheres with average diameters of 513 ± 24 and 602 ± 28 µm were reported using a CTP ceramic-to-polymer ratio of 10/3 and 20/3, respectively, whereas with HA the average diameters found were 429 ± 46 and 632 ± 40 µm for the same formulation.

Scanning electron microscopy (SEM) images indicated that these microspheres with average diameters of 0.9 μm were composed of SnO2 nanoparticles with a diameter of about 4.7 nm and a crystallite size of 3.7 nm, as observed by transmission electron microscope (TEM) and calculated by Scherrer's equation from diffractograms, respectively.

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Scanning electron microscopy (SEM) analysis indicates the formation of well-organized microspheres with an average diameter of 2 4 μm and transmission electron microscopy (TEM) images reveal LaFeO3 nanoparticles with an average size of 85 nm, which agrees well with the size obtained from XRD.

Hollow ZnO microspheres with an average diameter of ca. 2.7 μm were also obtained (Figure 1b).

Suspension of PMAA-PLA microspheres with an average size of 172.8 ± 3.6 nm was prepared with solvent evaporation technique.

The results show that the iron oxide/carbon composites consist of uniform microspheres with an average diameter of ∼2.1 μm.

When the molar ratio of EDTA was 1 mM, microspheres with an average length of 2.3 μm and diameter of 1.20 μm (Figure 2a) were obtained.

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