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Figure 3 Micro morphology of artificially aged silk sample before restoration.

Figure 4 Micro morphology of artificially aged silk sample after restoration.

Full characterizations regarding the structure, surface properties, and micro morphology of the material were performed.

The results showed that tensile strength, elongation rate at breakage and micro morphology of the silk samples were remarkably improved without significant colour difference after restoration.

However, the micro morphology of the gel underwent gel gel states changes via the stimuli of F− and recovered by the addition of H+.

The micro morphology of the original and worn surfaces obtained by scanning electron microscope was used to analyze the tribological mechanism.

In order to investigate the micro morphology of the artificially aged samples before and after restoration, scanning electron microscope images of the longitudinal section of the samples were observed.

The comparison between the micro morphology of the air-oil interface compared to the bulk phase volume has been studied even less.

X-ray diffraction (XRD), Fourier transform infrared pectroscopy (FTIR) and scanning electron microscope (SEM) have been used to investigate the phase composition and micro-morphologies of the products.

The PLLA microspheres were fabricated by the droplet-freezing process, the diameter and porosity of the microspheres were measured, and the micro-morphologies of the microspheres were characterized by scanning electron microscopy (SEM).

The micro-morphologies of the organogel were various, such as ellipsoids, spheres, cuboids and cylinders, and they could be obtained in sequence by controlling the stirring time or the dosage of introduced EtOH.